Solid Manure Sampling Procedures

Developing a nutrient management plan depends on testing manure for nutrient content. Your manure test results are only as good as your sample. This page outlines recommended ways to sample solid manure from open feedlots.

Sample During Loading

The recommended sampling for solid manure is to sample while loading the spreader. Sampling the manure pack in a barn directly has been shown to result in very variable results and is not recommended. Take at least 5 samples during the process of loading several spreader loads and save them in a bucket. When all of the samples are collected, thoroughly mix the samples and take a subsample from this to fill the lab manure test container.

Sample Manure During Spreading

Spread a tarp or sheet of plastic in the field and spread manure over this with the manure spreader. Do this in several locations and with several loads of manure. Collect the manure from the tarp or plastic sheet in a bucket. Mix the manure collected from different locations and spreaders, and take a subsample from this to fill the lab manure test container. This procedure is usually only practical for more solid manures.

Photo courtesy USDA NRCS

Sampling Daily Haul Manure

Place a 5 gallon bucket under the barn cleaner 4 or 5 times while loading the spreader. When all of the samples are collected, thoroughly mix the samples and take a subsample from this to fill the lab manure test container. Repeat this several times throughout the year to determine variability over time.

Sampling Manure in a Poultry House

Collect 8-10 samples from throughout the house to the depth of the litter to be removed. Samples near feeders and waterers can be very different. Collect samples from these areas proportional to the space they occupy in the house. When all of the samples are collected, thoroughly mix the samples and take a subsample from this to fill the lab manure test container. A sample taken while loading the spreader or during spreading is likely to be a more representative sample.

Sampling Stockpiled Litter

Take 10 samples from different locations around the pile at least 18 inches below the surface. When all of the samples are collected, thoroughly mix the samples and take a subsample from this to fill the lab manure test container. Large diameter auger bit and portable drill or soil sampler can be used to access manure deep within pile.

Taking a sample from a manure stockpile Taking representative sample from all subsamples mixed together in a bucket

Sampling stockpiled manure. Picture Source: Manure Testing for Nutrient Content

Sampling Manure from an Open Lot

These videos were produced by the Iowa Learning Farms project.

Sampling Stockpiled and Composted Manure

Related Web Pages

Overview of Manure Testing

Page Authors: Douglas Beegle, Penn State University and John Peters, University of Wisconsin

Liquid Manure Sampling Procedures

When testing manure, your nutrient management plan is only as good as your ability to obtain a representative sample. In liquid manure storage, agitation is critical to spreading uniform manure and to getting a representative sample. Agitating for 2-4 hours is the minimum. Depending on the type of storage longer agitation times may be required. The agitation for sampling should be similar to the agitation done when the storage is emptied. For this reason the most practical time to sample is when the storage is being emptied for field application.

If the storage is not adequately agitated there will likely be stratification. The figure below illustrates how manure analysis can vary within a storage without adequate agitation. In this example manure in the last 15 loads spread from this storage has 2 to 3 times more phosphorus than in the first 45 loads spread. If the storage is known to be stratified, separate samples should be taken as the manure consistency changes during emptying.

diagram

cc2.5 Les Lanyon

Sampling As Manure Storage Is Emptied

Agitate the storage thoroughly before sampling. Use a bucket to collect at least 5 samples during the process of loading several spreader loads and save them in the bucket. When all of the samples are collected, thoroughly mix the samples and take a subsample from this to fill the lab manure test container. When filling containers with liquid manure never fill the container more than ¾ full. If samples are collected over a several hour period, the bucket with manure sample should be stored on ice to limit ammonia losses.

Sample Manure When Pumping From Storage. Photo courtesy of Ontario Ministry of Agriculture, Food and Rural Affairs. Photo Source: http://www.thecattlesite.com/articles/1307/sampling-liquid-manure-for-analysis


Sampling From the Manure Storage

Picture Source: http://www.extension.iastate.edu/pages/communications/epc/Winter02/manure.html

Sampling a storage directly is much more difficult and likely to result in more variable results than sampling as the manure is loaded into the spreader. Agitate the storage thoroughly before sampling. Use a small bucket or tube to collect at least 5 samples from different locations in the storage. Combine these samples in a bucket and thoroughly mix the samples and take a subsample from this to fill the lab manure test container. When filling containers with liquid manure never fill the container more than ¾ full.

Liquid Manure Sampling Video

This video from the Iowa Learning Farms Project shows two sampling techniques for liquid manure storage prior to agitation. As indicated above, samples of agitated liquid manure should be obtained when possible, but in cases where the information from the lab analysis (which can take several days) is needed before manure can be applied to crop land.

Part 2: Sampling Liquid Manure

Sampling Manure During Application

This method is good for irrigated manure. Place buckets around the field to catch manure from the spreader or irrigation equipment. Place these to collect manure from more than one spreader load. Combine and mix the manure collected from different locations, and take a subsample from this to fill the lab manure test container. This method may give you “crop available ammonia nitrogen” as any ammonia losses may have already occurred prior to reaching bucket. What reaches the bucket is likely to soak into the soil and be available to the crop.

Related Web Pages

Overview of Manure Testing

Page Authors: Douglas Beegle, Penn State University and John Peters, University of Wisconsin